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1 article(s) from Klupp Taylor, Robin

Novel acridone-modified MCM-41 type silica: Synthesis, characterization and fluorescence tuning

Maximilian Hemgesberg,
Gunder Dörr,
Yvonne Schmitt,
Andreas Seifert,
Zhou Zhou,
Robin Klupp Taylor,
Sarah Bay,
Stefan Ernst,
Markus Gerhards,
Thomas J. J. Müller and
Werner R. Thiel

Beilstein J. Nanotechnol. 2011, 2, 284–292, doi:10.3762/bjnano.2.33

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Scheme 1: Synthesis of the sol–gel precursor 1.

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Figure 1: Infrared spectra of compound 1 (A), MCM-ACR (B) and MCM-ACR + Sc(OTf)₃ (C). The box marks the secti...

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Figure 2: C=O vibrational band section of the infrared spectra of compound 1 (A), MCM-ACR (B) and MCM-ACR + S...

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Figure 3: TEM images showing the mesoporous structure of MCM-ACR (left: frontal, right: lateral), inset in le...

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Figure 4: Sorption isotherm (left) and pore size distribution (BJH plot) (right) of MCM-ACR.

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Figure 5: XRD pattern of MCM-ACR.

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Figure 6: ¹³C CP-MAS NMR spectrum of MCM-ACR overlaid with the high resolution ¹³C NMR spectrum of precursor 1...

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Figure 7: ²⁹Si CP-MAS NMR spectrum of MCM-ACR.

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Figure 8: Visual appearance of MCM-ACR and MCM-ACR + Sc(OTf)₃ under normal (a) and UV light (b).

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Figure 9: Overlay of the solid state UV-vis (top) and fluorescence (bottom) spectra of MCM-ACR, MCM-ACR + Sc(...

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Full Research Paper

Published 09 Jun 2011

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